CHEM 322L Organic Chemistry II Laboratory
Syllabus
Andrea Drew Gounev, Ph.D. FH 510F, (816) 235-2257 drewa@umkc.edu
Lab Notebook Example
EXP. 1: X2 Addition to Alkenes: Bromination of trans-Stilbene
EXP. 1: Prelab Video
EXP. 1: Post Lab
EXP. 2: Epoxidation of Cholesterol
EXP. 2: Prelab Video & Video of Slurry (Wet-Loading) method for column packing and loading
EXP. 2: Post Lab
EXP. 3: Diels-Alder Reaction: Hexaphenylbenzene, Dimethyl tetraphenyl phthalate, 1,2,3,4-Tetraphenylnaphthalene
EXP. 3: Prelab Video
EXP. 3: Post Lab (You will be filling out and submitting along with your extended Experimental Section!)
EXP. 3: Powerpoint over Diels-Alder Reactions and Experimental Write-up-VERY HELPFUL!
EXP. 3: Video Lecture on the Experimental Section and a PDF Example of an Experimental Section!
EXP. 3: Video Lecture on the Diels-Alder Paper and a PDF Example of How to Write the Diels-Alder Paper! Example Citations or at http://www.lib.berkeley.edu/CHEM/acsstyle.html
EXP. 4: Diels-Alder Reaction: Triptycene
EXP. 4: Prelab Video
EXP. 4: Post Lab (You will be filling out and submitting along with your extended Experimental Section!)
EXP. 4: Reflux Apparatus
EXP. 4: Pressure Relieving Apparatus
EXP. 5: Acylation of Ferrocene
EXP. 5: Revised Ferrocene Instructions
EXP. 5: Prelab Video
EXP. 5: Post Lab
EXP. 6: Alkylation of Biphenyl and Para-Dimethoxybenzene
EXP. 6: Prelab Video
EXP. 6: Post Lab
EXP. 6: Preparation of the Water Trap in Part A
EXP. 7: Nitration of Methyl Benzoate
EXP. 7: Prelab Video
EXP. 7: Post Lab
EXP. 7: 1H NMR Spectrum of Methyl Benzoate IR Spectrum of Final Product
EXP. 8: Wittig Reaction
EXP. 8: Prelab Video
EXP. 8: Post Lab
EXP. 9: Aldol Condensation
EXP. 9: Prelab Video
EXP. 9: Post Lab
EXP. 10: Synthesis of Banana Oil
EXP. 10: Prelab Video
EXP. 10: Post Lab
EXP. 10: Distillation Apparatus (you can bring this to lab) IR Spectrum
EXAM Review
BLACKBOARD
