
Syllabus321L 
Coordinator of Organic Labs Andrea Drew Gounev, Ph.D. FH 510D, (816) 2352257 drewa@umkc.edu

Lab Bench Photo  
TA Office Hours  Standard Point Deductions  
Prelab Videos  Pictograms & Hazards  
EXP. 1: Crystallization: Recrystallization EXP. 1: Prelab Video EXP. 1: Post Lab 

EXP. 2: Distillation: Steam Distillation of Toluene – Benzil Mixture EXP. 2: Distillation Apparatus (You may bring this handout to lab!) EXP. 2: Prelab Video EXP. 2: Post Lab 

EXP. 3: Extraction I: Partition Coefficient and Separations of Acid/Neutral and Base/Neutral (complete steps AC during the first week), and Separation of Strong/Weak Acid (step D and any of AC not finished first week during the second week). (Note: this lab has been split into 2 different laboratory periods.) EXP. 3: Prelab Video EXP. 3: Post Lab 

EXP. 4: Extraction II: Separation and Purification of the Components of an Analgesic Tablet (Note: Experimental procedure must be written as a flowchart!) EXP. 4: Prelab Video EXP. 4: Post Lab 

EXP. 5: Extraction III: SolidLiquid Extraction: Trimyristin from Nutmeg EXP. 5: Reflux Apparatus (You may bring this handout to lab!) EXP. 5: Prelab Video EXP. 5: Post Lab 

EXP. 6: Grignard Reaction EXP. 6: Prelab Video EXP. 6: Post Lab EXP. 6: IR spectrum of triphenylmethanol 

EXP. 7: Substitution Reactions S_{N}2: Synthesis of trans1,2dibenzoylcyclopropane EXP. 7: Prelab Video EXP. 7: Post Lab 

EXP. 8: Substitution Reactions S_{N}1: triphenylmethanol EXP. 8: Prelab Video EXP. 8: Post Lab EXP. 8: Example of How to Write an Experimental Section! EXP. 8: J. Org Chem Guidelines for Authors from 2007 

EXP. 9: Elimination Reaction E1: Cyclohexene from cyclohexanol (fractional distillation) EXP. 9: IR spectra of cyclohexanol and cyclohexene EXP. 9: IR and NMR Handout EXP. 9: Prelab Video EXP. 9: Post Lab 

EXP. 10: Elimination Reaction E2: Cyclohexene from bromocyclohexane EXP. 10: Reflux Apparatus (You may bring this handout to lab!) EXP. 10: Distillation Apparatus (You may bring this handout to lab!) and Actual Photo EXP. 10: IR and NMR Handout EXP. 10: Prelab Video EXP. 10: Post Lab 
